Technical Activities

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"Technical Activities 2004" - Table of Contents

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Ionizing Radiation Division
The strategy for meeting this goal is to develop, maintain, and disseminate the national standards for ionizing radiation and radioactivity to meet national needs for health care, U.S. industry, and homeland security.
GOAL: To provide the
foundation of ionizing
radiation measurements
for our nation.

Strategic Focus Areas:

   

First

Radioactivity Standards  -  to develop and provide standards for radioactivity based on the SI unit, the becquerel, for homeland security, environmental, medical, and radiation protection applications.

Second

Neutron Standards and Measurements  -  to develop and provide neutron standards and measurements needed for fundamental physics, homeland security, the hydrogen economy, worker protection, and nuclear power.

Third

Radiation Dosimetry Standards  -  to develop dosimetric standards for x rays, gamma rays, and electrons based on the SI unit, the gray, for homeland security, medical, radiation processing, and radiation protection applications.


Neutron Standards and Measurements:

to develop and provide neutron standards and measurements needed for fundamental physics, homeland security, the hydrogen economy, worker protection, and nuclear power.

INTENDED OUTCOME AND BACKGROUND

The Neutron Interactions and Dosimetry Group provides measurement services, standards, and fundamental research in support of NIST's mission as it relates to neutron technology and neutron physics. The national interests served include industrial research and development, national defense, homeland security, higher education, electric power production, and more specifically, neutron imaging, scientific instrument calibration and development, neutron source calibration, detection of concealed nuclear materials, radiation protection, and nuclear and particle physics data.

The Group maintains and disseminates measurement standards for neutron dosimeters, neutron survey instruments, and neutron sources. The Group has initiated an accelerated program to develop effective neutron interrogation and measurement standards for national defense and homeland security needs, in collaboration with the Radioactivity Group.

The Group maintains and supports the Nation's premier fundamental neutron physics user facility. The Neutron Interferometry and Optics Facility is one of the most advanced user facilities of this kind in the world. The Group's neutron interferometry program provides the world's most accurate measurements of neutron coherent scattering lengths, important to materials science research and modeling of the nuclear potentials. Preparations for new neutron interferometry experiments for surface studies of multilayers, for determination of the charge distribution in the neutron, and for investigation of quantum information/coherence phenomena are being carried out.

The Group is at the forefront of basic research with neutrons in the measurements of symmetries and parameters of the weak nuclear interactions, addressing fundamental issues that are important in the understanding of theories of evolution of the cosmos. It is an internationally renowned program that maintains an extensive level of cooperation with premier national and international academic and research institutions.

We have developed and we maintain the Nation's only high-resolution neutron imaging user facility. It is available for both proprietary and open research at the NIST Center for Neutron Research (NCNR). Research at this facility is primarily dedicated to applying neutron imaging methods for industrial research on water transport in fuel cells and on hydrogen distribution in hydrogen storage devices. Neutron imaging, vigorously pursued by the Group, has rapidly developed to be the technique of choice for nondestructive, in situ water transport studies in PEM-type fuel cells. This facility has provided critical services to major automotive and fuel cell companies, and continues to be in high demand.

The Group is also among the world leaders in developing 3He-based neutron polarization and analysis techniques. We are developing and promoting the applications of neutron spin filters based on laser-polarized 3He. The technique has the unique capability to polarize a polychromatic neutron beam without introducing additional beam divergence. This is a very attractive feature for many materials science and fundamental physics applications. We are pursuing applications at the NCNR, the Intense Pulsed Neutron Source (IPNS) at Argonne National Laboratory, and the Los Alamos Neutron Science Center.

Accomplishments

  • Neutron Technology for Homeland Security

    We have participated in the development of three new ANSI Standards, N42.32, N42.34, and N42.35, which provide test and evaluation protocols for neutron detection in personal electronic radiation monitors ("pagers"), isotope identifier instruments, and portal monitors, respectively. We are managing the procurement, calibration, and dissemination of standard, low-intensity neutron sources to three national laboratories for testing of commercial instruments under these standards. We are also leading the development of new, additional ANSI standards on neutron survey meters and active interrogation devices for detection of fissile material, explosives, and chemical agents.

    The challenge of calibrating low-intensity sources has motivated the development of a new source comparator with a reduced-volume manganese sulfate bath. For measurement of neutron radiation protection levels around active interrogation devices, we have procured and calibrated state-of-the-art commercial neutron spectrometry and absorbed-dose measurement systems.

    We are developing neutron spectrometers and epithermal/thermal neutron detectors with much higher sensitivity than current state-of-the-art systems. We are experimenting with muon anticoincidence techniques for reducing the cosmic-ray component of neutron background radiation. Finally, we have procured and calibrated a small, sealed-tube source for generating 14 MeV and 2.5 MeV fast neutrons, for testing our new spectroscopy systems, and for developing radiation-protection dosimetry capabilities up to 14 MeV.


    CONTACT: Dr. David M. Gilliam
    (301) 975-6206
    david.gilliam@nist.gov



  • New Imaging Station for Fuel Cell Research

    The Neutron Imaging Facility started full-time operation in 2003 at Beam Tube 6 (BT-6) at the NCNR. The facility has an extremely high fluence rate of 1.8 × 107 cm-2 s-1 uniformly spread over a 26 cm diameter area, with an L/d ratio of 300, which is needed to achieve optimum geometric sharpness of the image. This is one of the most advanced neutron imaging facilities in the world and the best of its kind in the U.S.

    We have pioneered nondestructive imaging techniques to map critically important hydrogen and water motion in operating fuel cells. This facility has been hosting experiments from industrial fuel cell developers, interested in looking at the distribution of water in operational fuel cell systems using standard fuel cell hardware. First-generation neutron experiments with a major industrial partner show exciting promise of robust/efficient fuel cell design, substantial reduction in fuel cell development time, and establishment of uniform characterization/performance standards.

    This program has been awarded NIST competence research funding and, in 2003, DOE recognized this program as one of the top-ten programs relevant to the "FreedomCAR" program initiated by the President.


    CONTACT: Dr. David L. Jacobson
    (301) 975-6207
    david.jacobson@nist.gov



  • Neutron Measurements to Test "Standard Model"

      Figure 3

    Figure 3. Pieter Mumm (second from right) and colleagues setting up a neutron decay detector for the time reversal asymmetry experiment (emiT).


    The emiT experiment successfully completed its data acquisition on NG-6 in December 2003. (See Fig. 3.) The experiment is a collaboration among NIST, the University of Washington, the University of California (Berkeley), the University of Michigan, Hamilton College, and Tulane University.

    The experiment searches for (or will set an improved upper bound on) the time-reversal asymmetry term in neutron beta decay. It does so by measuring electron-proton coincidence events from the decay of polarized neutrons. An asymmetry in coincidence pairs is formed as a function of the direction of the neutron spin. A measurement of a nonzero asymmetry would be an indication of time-reversal violation.

    The measured electron-proton coincidence rate is a factor-of-ten higher than in the first run. In addition, the signal-to-background ratio is two orders of magnitude higher. The analysis of the data is in progress, and we anticipate a result that is approximately a factor of four better than the world current limit.

    Work has commenced at NG-6 on an effort to measure the radiative decay mode of the free neutron. The usual beta decay of the neutron into a proton, electron, and antineutrino is occasionally accompanied by the emission of a photon. Despite decades of detailed experimental studies of neutron beta decay, this branch of a fundamental weak decay has never been observed.

    Our technique is based on measuring the triple coincidence of the proton and electron along with the rare photon. The experiment should not only definitively see radiative neutron beta decay for the first time, but also perform a 5 % measurement of the photon spectrum.


    CONTACT: Dr. Jeffery S. Nico
    (301) 975-4663
    jeffrey.nico@nist.gov



  • Polarized 3He Neutron Spin Filters for Fundamental and Applied Research

      Figure 4

    Figure 4. Polarization analysis of neutron reflection from a sample of cobalt "antidots," obtained with a 3He analyzer and a position-sensitive detector. Qz and Qx are the z and x components of the wavevector transfer; spin-flip scattering from magnetic domains is evident in the off-specular data.

    In collaboration with scientists in the NIST Materials Science and Engineering Laboratory and Indiana University, we are employing 3He-based polarization analysis for diffuse reflectometry at the new Advanced Neutron Diffractometer/Reflectometer at the NCNR, and the POSY-I reflectometer at IPNS.

    Our current focus is on studies of patterned magnetic materials, which are relevant to the development of future magnetic storage media (Fig. 4). In addition, we are collaborating with researchers from Hamilton College, IPNS, and the Spallation Neutron Source in the application of a continuously operating 3He polarizer for single-crystal diffractometry.

    In fundamental physics, we are contributing to the operation and further development of the 3He polarizer for an experiment in weak interaction physics (the "npdγ" experiment) at Los Alamos National Laboratory. In addition, we are developing 3He cells for a planned measurement of the spin dependence of the 3He scattering length on the NCNR neutron interferometer. In collaboration with the University of Utah, we have documented remarkable magnetic effects in the polarized 3He storage cells, which are relevant to suppressing wall relaxation time.


    CONTACT: Dr. Thomas R. Gentile
    (301) 975-5431
    thomas.gentile@nist.gov


First strategic focus   |   Second strategic focus   |   Third strategic focus

"Technical Activities 2004" - Table of Contents